Volume : 2, Issue : 4, APR 2016
METHODS OF GROWING SINGLE CRYSTALS
Nazia Siddiqui, Saleem Javed
Abstract
In the synthesis (organic, inorganic, organometallic, biochemical) crystal structure of the compound is the milestone. Any crystal structure shows - exact connectivity,bond distances, angles, complete identification of the compound, intermolecular interactions and intramolecular interactions. Information gained is rarely incorrect. It provides positive identification and answers of basic questions regarding bonding. To know the crystal structure we have to grow single crystals by using different strategies and have the idea how single crystals grow from solid, liquid and gas phase.
Keywords
Crystal growth, single crystal, data collection, structure refinement
Article : Download PDF
Cite This Article
Article No : 26
Number of Downloads : 974
References
1. Müller, P., Herbst-Irmer, R., Spek, A.L., Schneider, T.R., Sawaya, M.R. (2006) Crystal
Structure Refinement A Crystallographer's Guide to SHELXL; Oxford University
Press: Oxford, UK, 2006.
2. Clegg, W., Blake, A. J., Gould, R.O., Main, P. (2001) Crystal Structure Analysis Principles
and Practice; Oxford University Press: Oxford, UK, 2001.
3. Herbst-Irmer, R., Sheldrick, G.M. (1998) Refinement of Twinned Structures with
SHELXL97. Acta Crystallogr, B54, PP. 443–449.
4. Herbst-Irmer, R., Sheldrick, G.M., (2002) Refinement of Obverse/Reverse Twins.
Acta Crystallogr, B58, PP. 477-481.
5. Watkin, D.J., (1994) The Control of Difficult Refinements. Acta Crystallogr, A50, PP.
411–437.
6. Sheldrick, G.M., (2008) A Short History of SHELX. Acta Crystallogr, A64, PP.
112–122.
7. Watkin, D.J., (2008) Structure Refinement: Some Background Theory and Practical
Strategies. J. Appl.Crystallogr, 41, PP. 491–522.
8. http://www.xtal.iqfr.csic.es/Cristalografia/parte_10_1-en.html
9. Peter, G. J., (1981) Crystal Growing, Chemistry in Britain, 17, PP. 222-225
10. Siddiqui, N., Sangeeta, Javed, S., (2016), Single Crystal Crystallography: Crystal
Growth and Design, EMOTBAS- 2016, Submitted